Sediment cores were collected from the East Antarctic margin, aboard the Australian Marine National Facility R/V Investigator from January 14th to March 5th 2017 (IN2017_V01; (Armand et al., 2018). This marine geoscience expedition, named the “Sabrina Sea Floor Survey”, focused notably on studying the interactions of the Totten Glacier with the Southern Ocean through multiple glacial cycles. The cores were collected using a multi-corer (MC), were sliced every centimetre, wrapped up in plastic bags, and stored in the fridge. Sediment samples were dried in an oven at 40°C and ground using a pestle and a mortar. Biogenic silica (or ‘opal’) analysis was carried out following modification of the protocol of Mortlock and Froelich (1989). About 30 mg of sediment was leached with 30 mL of 1M sodium carbonate (Na2CO3) for 5 hours at 80°C. Every hour, 1 mL of sample was removed and centrifuged at 10,000 rpm for 30 sec. A 200 µL aliquot was removed from the supernatant and diluted 50x with Milli-Q water for SiO2 determination by molybdate-blue spectrophotometry. A standard calibration was prepared by dilution of a SiO2 standard solution (sodium hexafluorosilicate, from 0 to 200 µM). The opal concentrations were calculated using the slope of the last three points of the dissolution curve (Demaster, 1981), or the changing slope part of the curve. References - Armand, L. K., O’Brien, P. E., Armbrecht, L., Baker, H., Caburlotto, A., Connell, T., … Young, A. (2018). Interactions of the Totten Glacier with the Southern Ocean through multiple glacial cycles (IN2017-V01): Post-survey report. ANU Research Publications. - Demaster, D. J. (1981). The supply and accumulation of silica in the marine environment. Geochimica et Cosmochimica Acta, 45, 1715–1732. - Mortlock, R. A., and Froelich, P. N. (1989). A simple method for the rapid determination of biogenic opal in pelagic marine sediments. Deep-Sea Research Part I, 36(9), 1415–1426.

Detailed sedimentary information and palaeontological samples were collected from Battye Glacier Formation, of the Pagodroma Group in the Prince Charles Mountains, an area where little information is presently available. The mid to Upper Cenozoic Pagodroma Group provides direct evidence for past changes in climate and glacial environments from deep within the Antarctic continent. Evidence from several geological formations in the Pagodroma Group, many of them fossil-bearing, will help to determine the history of fluctuations in climate and the size of the East Antarctic Ice Sheet (EAIS). This will provide baseline data to help validate the predictive numerical models of ice sheet dynamics. There is a clear need to study the response of the EAIS to past times of global warming. Periods of significance include times when atmospheric CO2 levels were similar to today (Poore and Sloan 1996). Another key time interval is during the late Neogene, prior to the development of Northern Hemisphere glaciation, which has largely governed Antarctic Ice Sheet volume changes during the Quaternary (Clapperton and Sugden 1990; Mabin 1990; Huybrechts 1990, 1992). An important aspect of the research is to build onto the geological data-set collected by ODP Leg 119, 120 and 188 in Prydz Bay. These operations have concentrated on the periphery of Antarctica and, therefore, record ice sheet retreat and advance at its outer-limits. The Pagodroma Group provides significant information about ice sheet variation at its the inner reaches. Together, these data-sets will shape our understanding of major fluctuations of the ice sheet through the Cenozoic, and will assist and test the models developed to predict ice sheet behavior in the future. Direct geological evidence for climatic conditions and the extent of the ice sheet during times of glacial retreat can be obtained only from onshore geological records, such as the Pagodroma Group. This is important given the current warming trends, expected ice sheet retreat and global sea-level rise, and general lack of geological data from onshore Antarctica for predicting the effects of this on the EAIS. Fieldwork was conducted during November - December (2000). A number of significant findings were made from the Amery Oasis: 1) New outcrops of the glacio-marine Battye Glacier Formation were located and mapped. Up to 800 m of geological section was logged and sampled. Similar Antarctic records have only been made available through expensive international drilling efforts around the Antarctic shelf. This project highlights that there are extensive records exposed on land, that can be studied for a fraction of the cost of off-shore marine geoscience. 2) Unique diatomaceous marine mudstone deposits were discovered (~9 m thick). This is the most diatomaceous (up to 12% biogenic silica), in situ marine deposit that has have been found from inland Antarctica. Diatom biostratigraphy indicates that the formation is middle - late Miocene in age. 3) In situ and articulate marine mollusc fossil horizons were discovered. These occur over a lateral distance of ~ 1km and provide undisputable evidence for a major ice sheet retreat in the past. 4) Three erratics containing marine mollusc fossils were discovered. These erratic are potentially Cretaceous in age (Stilwell, pers. comm.). This is the first marine sediment of this age found in the Lambert Graben catchment. Eleven pdf figures are available for download from the provided URL. Also included is a text file which explains what each of the figures are. Furthermore, two excel spreadsheets of data are also available. The two excel spreadsheets in the download directly relate to the paper Whitehead, et al (2003). Some explanatory notes for the excel files are: Qualitative assessment of fossil preservation vf = very fragmented with a few intact specimens seen per traverse of a microscope slide. mf = moderately fragmented with an intact specimen seen every few fields of view (at 600x magnification). See Whitehead et al (2003) for more information. Qualitative fossil abundance, where X = (present) one valve (Diatom valves)/fossil seen during entire examination. R = (rare) greater than 3 valves/fossils seen during all microscope traverses on slide. F = (few) greater than 1 valve/fossil per 10 microscope fields of view (at 600x magnification). C = (common) valves/fossils in each microscope field of view (at 600x magnification). The fields in this dataset are: Stratigraphic Intervals Samples Opal% McLeod Beds Bed A clasts Fossil Preservation Benthic Diatom Abundance Species Bardin Bluffs Formation Fisher Bench Formation Diatoms