Opal concentrations measured in sediment samples collected during the IN2017-V01 voyage of the RV Investigator

Sediment cores were collected from the East Antarctic margin, aboard the Australian Marine National Facility R/V Investigator from January 14th to March 5th 2017 (IN2017_V01; (Armand et al., 2018). This marine geoscience expedition, named the “Sabrina Sea Floor Survey”, focused notably on studying the interactions of the Totten Glacier with the Southern Ocean through multiple glacial cycles. The cores were collected using a multi-corer (MC), were sliced every centimetre, wrapped up in plastic bags, and stored in the fridge.

Sediment samples were dried in an oven at 40°C and ground using a pestle and a mortar. Biogenic silica (or ‘opal’) analysis was carried out following modification of the protocol of Mortlock and Froelich (1989). About 30 mg of sediment was leached with 30 mL of 1M sodium carbonate (Na2CO3) for 5 hours at 80°C. Every hour, 1 mL of sample was removed and centrifuged at 10,000 rpm for 30 sec. A 200 µL aliquot was removed from the supernatant and diluted 50x with Milli-Q water for SiO2 determination by molybdate-blue spectrophotometry. A standard calibration was prepared by dilution of a SiO2 standard solution (sodium hexafluorosilicate, from 0 to 200 µM). The opal concentrations were calculated using the slope of the last three points of the dissolution curve (Demaster, 1981), or the changing slope part of the curve.

References

- Armand, L. K., O’Brien, P. E., Armbrecht, L., Baker, H., Caburlotto, A., Connell, T., … Young, A. (2018). Interactions of the Totten Glacier with the Southern Ocean through multiple glacial cycles (IN2017-V01): Post-survey report. ANU Research Publications.

- Demaster, D. J. (1981). The supply and accumulation of silica in the marine environment. Geochimica et Cosmochimica Acta, 45, 1715–1732.

- Mortlock, R. A., and Froelich, P. N. (1989). A simple method for the rapid determination of biogenic opal in pelagic marine sediments. Deep-Sea Research Part I, 36(9), 1415–1426.

Identification info

Alternate title: Opal concentrations measured in sediment samples collected during the IN2017-V01 voyage of the RV Investigator

Date (Publication): 2023-04-03

Edition: 1

Citation identifier

Dataset DOI

Title: Information and documentation - Digital object identifier system

Date (Publication): 2012-04-23

Citation identifier: ISO 26324:2012

Citation identifier: doi:10.26179/paed-e557

Originator

Creac'h, L., Noble, T.L. and Durand, A.

Publisher

Australian Antarctic Data Centre

Principal investigator

CREAC'H, LAYLA

Institute for Marine and Antarctic Studies

20 Castray Esplanade, Battery Point

Hobart

TAS

7004

Australia

Principal investigator

NOBLE, TARYN L

Institute of Marine and Antarctic Studies

20 Castray Esplanade

Hobart

Tas

7004

Australia

Collaborator

CREAC'H, LAYLA

Institute for Marine and Antarctic Studies

20 Castray Esplanade, Battery Point

Hobart

TAS

7004

Australia

Collaborator

DURAND, AXEL

Institute for Marine and Antarctic Studies

20 Castray Esplanade, Battery Point

Hobart

TAS

7004

Australia

Name: CAASM Metadata

Other citation details: Unreleased data

Website: https://data.aad.gov.au/metadata/records/AAS_4419_opal_sediment_MC

Purpose: These data were collected in order to determine the opal content of marine sediment from Wilkes Land margin, to reconstruct past productivity.

Status: Completed

Custodian

AU/AADC > Australian Antarctic Data Centre, Australia - AADC, DATA OFFICER (DATA CENTRE CONTACT)

Australian Antarctic Division

203 Channel Highway

Kingston

Tasmania

7050

Australia

+61 3 6232 3244

+61 3 6232 3351 (facsimile)

Topic category

Oceans

Extent